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Information card for entry 7014136
Preview
Coordinates | 7014136.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H33 Cl2 N2 Ni O4 P |
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Calculated formula | C22 H33 Cl2 N2 Ni O4 P |
Title of publication | Nickel and iron complexes with oxazoline- or pyridine-phosphonite ligands; synthesis, structure and application for the catalytic oligomerisation of ethylene. |
Authors of publication | Speiser, Fredy; Braunstein, Pierre; Saussine, Lucien |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2004 |
Journal issue | 10 |
Pages of publication | 1539 - 1545 |
a | 18.2474 ± 0.0006 Å |
b | 9.4918 ± 0.0002 Å |
c | 15.6567 ± 0.0007 Å |
α | 90° |
β | 102.837 ± 0.005° |
γ | 90° |
Cell volume | 2643.97 ± 0.17 Å3 |
Cell temperature | 294 K |
Ambient diffraction temperature | 294 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.062 |
Residual factor for significantly intense reflections | 0.033 |
Weighted residual factors for all reflections | 0.107 |
Weighted residual factors for all reflections included in the refinement | 0.048 |
Goodness-of-fit parameter for all reflections | 1.242 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | Mo-Kα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7014136.html
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