Information card for entry 7014257

Structure parameters

• Formula: C33 H42 Cl2 N4 Sn2
• Calculated formula: C33 H42 Cl2 N4 Sn2
• Title of publication: Synthesis and structures of beta-diketiminatotin(II) halides, an amide and of Sn(=E)[{N(R)C(Ph)}2CH](NR2) (E = S or Se, R = SiMe3).
• Authors of publication: Hitchcock, Peter B.; Hu, Jin; Lappert, Michael F.; Severn, John R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 24
• Pages of publication: 4193 - 4201
• a: 11.28 ± 0.006 Å
• b: 25.044 ± 0.012 Å
• c: 12.767 ± 0.008 Å
• α: 90°
• β: 107.19 ± 0.03°
• γ: 90°
• Cell volume: 3446 ± 3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1065
• Residual factor for significantly intense reflections: 0.0738
• Weighted residual factors for significantly intense reflections: 0.1766
• Weighted residual factors for all reflections included in the refinement: 0.1987
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No