Information card for entry 7014259

Structure parameters

• Formula: C27 H47 N3 S Si4 Sn
• Calculated formula: C27 H47 N3 S Si4 Sn
• SMILES: [Sn]1(=S)([N]([Si](C)(C)C)=C(C=C(N1[Si](C)(C)C)c1ccccc1)c1ccccc1)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Synthesis and structures of beta-diketiminatotin(II) halides, an amide and of Sn(=E)[{N(R)C(Ph)}2CH](NR2) (E = S or Se, R = SiMe3).
• Authors of publication: Hitchcock, Peter B.; Hu, Jin; Lappert, Michael F.; Severn, John R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 24
• Pages of publication: 4193 - 4201
• a: 18.795 ± 0.005 Å
• b: 8.974 ± 0.006 Å
• c: 21.617 ± 0.003 Å
• α: 90°
• β: 105.82 ± 0.02°
• γ: 90°
• Cell volume: 3508 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0726
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.0802
• Weighted residual factors for all reflections included in the refinement: 0.0916
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No