Information card for entry 7014387

Structure parameters

• Formula: C21 H54 Mo N3 O3 P Si3
• Calculated formula: C21 H54 Mo N3 O3 P Si3
• Title of publication: Reactions of trialkoxynitridomolybdenum with low-coordinate phosphorus compounds containing a P=N double bond.
• Authors of publication: Kovalenko, Oleksandr O.; Boldog, Ishtvan; Kinzhybalo, Vasyl; Lis, Tadeusz; Brusilovets, Anatolii I.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 3
• Pages of publication: 711 - 717
• a: 9.865 ± 0.003 Å
• b: 17.714 ± 0.005 Å
• c: 20.325 ± 0.006 Å
• α: 70.65 ± 0.03°
• β: 77.37 ± 0.03°
• γ: 88.48 ± 0.03°
• Cell volume: 3266 ± 1.8 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1086
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for significantly intense reflections: 0.0703
• Weighted residual factors for all reflections included in the refinement: 0.0792
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No