Information card for entry 7014636

Structure parameters

• Formula: C59.5 H87.5 Cl3 N Nb O3
• Calculated formula: C59.5 H68 Cl3 N Nb O3
• Title of publication: Synthesis and reactivity of niobium complexes having a tripodal triaryloxide ligand in bidentate, tridentate, and tetradentate coordination modes.
• Authors of publication: Akagi, Fumio; Ishida, Yutaka; Matsuo, Tsukasa; Kawaguchi, Hiroyuki
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 10
• Pages of publication: 2375 - 2382
• a: 13.987 ± 0.006 Å
• b: 20.447 ± 0.008 Å
• c: 21.538 ± 0.009 Å
• α: 94.951 ± 0.006°
• β: 99.947 ± 0.005°
• γ: 97.388 ± 0.007°
• Cell volume: 5979 ± 4 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0658
• Weighted residual factors for all reflections included in the refinement: 0.152
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No