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Information card for entry 7014693
Preview
Coordinates | 7014693.cif |
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Original paper (by DOI) | HTML |
Formula | C53 H59 N2 V |
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Calculated formula | C53 H59 N2 V |
SMILES | [V]123456([N](c7c(C(C)C)cccc7C(C)C)=C(C)C=C(N1c1c(C(C)C)cccc1C(C)C)C)[cH]1[c]2([cH]3[c]4([cH]5[c]61c1ccccc1)c1ccccc1)c1ccccc1 |
Title of publication | Ligand-controlled synthesis of vanadium(i) β-diketiminates and their catalysis in cyclotrimerization of alkynes. |
Authors of publication | Chang, Kai-Chieh; Lu, Chia-Fu; Wang, Po-Yang; Lu, Duan-Yen; Chen, Hong-Zhang; Kuo, Ting-Shen; Tsai, Yi-Chou |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 10 |
Pages of publication | 2324 - 2331 |
a | 13.2728 ± 0.0011 Å |
b | 13.3879 ± 0.0011 Å |
c | 14.0552 ± 0.0012 Å |
α | 98.915 ± 0.003° |
β | 117.457 ± 0.004° |
γ | 92.696 ± 0.003° |
Cell volume | 2169.3 ± 0.3 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.2764 |
Residual factor for significantly intense reflections | 0.1177 |
Weighted residual factors for significantly intense reflections | 0.2258 |
Weighted residual factors for all reflections included in the refinement | 0.305 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7014693.html
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Users of the data should acknowledge the original authors of the
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