Information card for entry 7014893

Structure parameters

• Formula: H74 Mn4 O105 V2 W19 Zn3
• Calculated formula: Mn4 O105 V2 W19 Zn3
• Title of publication: The synergistic effect of [WZn(VO)2(ZnW9O34)2]12- cores and peripheral metal sites in catalytic oxidative cyclization of acetylacetone.
• Authors of publication: Shi, Lian-Xu; Zhang, Xian-Wei; Wu, Chuan-De
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 4
• Pages of publication: 779 - 781
• a: 12.5382 ± 0.0003 Å
• b: 13.9382 ± 0.0004 Å
• c: 16.7244 ± 0.0005 Å
• α: 84.004 ± 0.002°
• β: 73.969 ± 0.002°
• γ: 63.604 ± 0.003°
• Cell volume: 2515.66 ± 0.14 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1143
• Residual factor for significantly intense reflections: 0.0967
• Weighted residual factors for significantly intense reflections: 0.2451
• Weighted residual factors for all reflections included in the refinement: 0.2512
• Goodness-of-fit parameter for all reflections included in the refinement: 1.332
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No