Information card for entry 7014895

Structure parameters

• Formula: H98 K2 Ni4 O118 V2 W19 Zn3
• Calculated formula: K2 Ni4 O118 V2 W19 Zn3
• Title of publication: The synergistic effect of [WZn(VO)2(ZnW9O34)2]12- cores and peripheral metal sites in catalytic oxidative cyclization of acetylacetone.
• Authors of publication: Shi, Lian-Xu; Zhang, Xian-Wei; Wu, Chuan-De
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 4
• Pages of publication: 779 - 781
• a: 32.1482 ± 0.0009 Å
• b: 14.5862 ± 0.0004 Å
• c: 21.7639 ± 0.0006 Å
• α: 90°
• β: 96.069 ± 0.002°
• γ: 90°
• Cell volume: 10148.3 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0794
• Residual factor for significantly intense reflections: 0.0649
• Weighted residual factors for significantly intense reflections: 0.1604
• Weighted residual factors for all reflections included in the refinement: 0.1646
• Goodness-of-fit parameter for all reflections included in the refinement: 1.15
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No