Information card for entry 7015015

Structure parameters

• Formula: C21.6 H28.4 F6 N2 O7 Rh Sb
• Calculated formula: C12 H6 F6 N2 O4 Rh Sb
• Title of publication: First metal complexes of 6,6'-dihydroxy-2,2'-bipyridine: from molecular wires to applications in carbonylation catalysis.
• Authors of publication: Conifer, Christopher M.; Taylor, Russell A.; Law, David J.; Sunley, Glenn J.; White, Andrew J. P.; Britovsek, George J. P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 5
• Pages of publication: 1031 - 1033
• a: 16.5179 ± 0.0005 Å
• b: 18.8624 ± 0.0006 Å
• c: 24.3868 ± 0.0007 Å
• α: 97.653 ± 0.003°
• β: 98.711 ± 0.003°
• γ: 109.593 ± 0.003°
• Cell volume: 6936.2 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0975
• Residual factor for significantly intense reflections: 0.0507
• Weighted residual factors for significantly intense reflections: 0.1193
• Weighted residual factors for all reflections included in the refinement: 0.1305
• Goodness-of-fit parameter for all reflections included in the refinement: 0.785
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No