Information card for entry 7015094

Structure parameters

• Formula: C55 H52 B2 Cl6 N12 P2 Ru2
• Calculated formula: C55 H52 B2 Cl6 N12 P2 Ru2
• Title of publication: Proton-induced reactivities of ruthenium azido complexes: the first example of boron-carbon bond formation by methylene insertion into a B-H bond.
• Authors of publication: Lo, Yih-Hsing; Chen, Han-Gung; Kuo, Ting Shen
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 12
• Pages of publication: 2711 - 2715
• a: 9.396 ± 0.0002 Å
• b: 16.921 ± 0.0004 Å
• c: 19.5683 ± 0.0004 Å
• α: 76.967 ± 0.001°
• β: 85.209 ± 0.001°
• γ: 75.117 ± 0.001°
• Cell volume: 2928.25 ± 0.11 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.0981
• Weighted residual factors for all reflections included in the refinement: 0.1046
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No