Information card for entry 7015267

Structure parameters

• Formula: C30 H42 N2 Ni O7
• Calculated formula: C30 H42 N2 Ni O7
• Title of publication: Access to multinuclear salen complexes using olefin metathesis.
• Authors of publication: Haak, Robert M.; Castilla, Ana M.; Belmonte, Marta Martínez; Escudero-Adán, Eduardo C; Benet-Buchholz, Jordi; Kleij, Arjan W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 13
• Pages of publication: 3352 - 3364
• a: 8.32 ± 0.0004 Å
• b: 13.9529 ± 0.0008 Å
• c: 14.0274 ± 0.0008 Å
• α: 112.341 ± 0.001°
• β: 100.392 ± 0.002°
• γ: 94.466 ± 0.002°
• Cell volume: 1462.16 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0416
• Residual factor for significantly intense reflections: 0.0358
• Weighted residual factors for significantly intense reflections: 0.1018
• Weighted residual factors for all reflections included in the refinement: 0.1063
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No