Crystallography Open Database

Information card for entry 7015284

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Coordinates	7015284.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 N28 Ni3 W2
Calculated formula	C46 N28 Ni3 W2
Title of publication	Microporous {[Ni(cyclam)]3[W(CN)8]2}n affording reversible structural and magnetic conversions.
Authors of publication	Nowicka, Beata; Bałanda, Maria; Gaweł, Bartłomiej; Ćwiak, Grzegorz; Budziak, Andrzej; Łasocha, Wiesław; Sieklucka, Barbara
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2011
Journal volume	40
Journal issue	12
Pages of publication	3067 - 3073
a	9.163 ± 0.002 Å
b	14.894 ± 0.005 Å
c	16.304 ± 0.005 Å
α	73.65 ± 0.03°
β	92.59 ± 0.03°
γ	90.67 ± 0.03°
Cell volume	2132.9 ± 1.1 Å³
Cell temperature	293 K
Ambient diffraction temperature	293 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.28
Weighted residual factors for significantly intense reflections	0.2778
RFsqd	0.23
Goodness-of-fit parameter for all reflections	2.48
Method of determination	powder diffraction
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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