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Information card for entry 7015295
Preview
Coordinates | 7015295.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H32 N4 O8 Zn2 |
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Calculated formula | C28 H32 N4 O8 Zn2 |
Title of publication | Zinc(ii) ortho-hydroxyphenylhydrazo-β-diketonate complexes and their catalytic ability towards diastereoselective nitroaldol (Henry) reaction. |
Authors of publication | Kopylovich, Maximilian N.; Mac Leod, Tatiana C. O.; Mahmudov, Kamran T.; Guedes da Silva, M Fátima C; Pombeiro, Armando J. L. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 19 |
Pages of publication | 5352 - 5361 |
a | 6.8688 ± 0.0003 Å |
b | 9.8233 ± 0.0005 Å |
c | 11.9184 ± 0.0006 Å |
α | 106.825 ± 0.002° |
β | 105.369 ± 0.003° |
γ | 95.625 ± 0.002° |
Cell volume | 728.81 ± 0.06 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0482 |
Residual factor for significantly intense reflections | 0.0359 |
Weighted residual factors for significantly intense reflections | 0.0819 |
Weighted residual factors for all reflections included in the refinement | 0.087 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7015295.html
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