Information card for entry 7015467

Structure parameters

• Formula: C54 H108 O13 P Rh Si8
• Calculated formula: C54 H108 O13 P Rh Si8
• Title of publication: Silsesquioxyl rhodium(I) complexes‒synthesis, structure and catalytic activity.
• Authors of publication: Marciniec, Bogdan; Kownacki, Ireneusz; Franczyk, Adrian; Kubicki, Maciej
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 18
• Pages of publication: 5073 - 5077
• a: 10.9023 ± 0.0012 Å
• b: 14.8954 ± 0.0018 Å
• c: 21.769 ± 0.003 Å
• α: 99.731 ± 0.012°
• β: 98.469 ± 0.009°
• γ: 104.467 ± 0.01°
• Cell volume: 3306.6 ± 0.8 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0958
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.1313
• Weighted residual factors for all reflections included in the refinement: 0.1368
• Goodness-of-fit parameter for all reflections included in the refinement: 0.96
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No