Information card for entry 7015479

Structure parameters

• Formula: C38 H54 Cl2 N3 O2 V
• Calculated formula: C38 H54 Cl2 N3 O2 V
• Title of publication: Synthesis of vanadium(III) complexes bearing iminopyrrolyl ligands and their role as thermal robust ethylene (co)polymerization catalysts.
• Authors of publication: Mu, Jing-Shan; Wang, Yong-Xia; Li, Bai-Xiang; Li, Yue-Sheng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 14
• Pages of publication: 3490 - 3497
• a: 9.3696 ± 0.0007 Å
• b: 15.8826 ± 0.0012 Å
• c: 16.5052 ± 0.0013 Å
• α: 95.561 ± 0.001°
• β: 106.305 ± 0.001°
• γ: 90.222 ± 0.001°
• Cell volume: 2345.1 ± 0.3 ų
• Cell temperature: 185 ± 2 K
• Ambient diffraction temperature: 185 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0706
• Residual factor for significantly intense reflections: 0.0492
• Weighted residual factors for significantly intense reflections: 0.1194
• Weighted residual factors for all reflections included in the refinement: 0.1289
• Goodness-of-fit parameter for all reflections included in the refinement: 0.982
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No