Information card for entry 7015550

Structure parameters

• Formula: C55.04 H52.08 Al N3 O0.26 P2
• Calculated formula: C55 H52 Al N3 O0.25 P2
• Title of publication: Dimethylaluminium iminophosphoranylenamides and iminophosphoranylanilides: synthesis, characterisation, and their controlled ring-opening polymerisation of ε-caprolactone.
• Authors of publication: Ma, Wen-An; Wang, Li; Wang, Zhong-Xia
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 17
• Pages of publication: 4669 - 4677
• a: 10.7891 ± 0.0012 Å
• b: 15.4618 ± 0.0014 Å
• c: 17.1493 ± 0.0018 Å
• α: 63.402 ± 0.008°
• β: 72.448 ± 0.009°
• γ: 89.894 ± 0.009°
• Cell volume: 2409 ± 0.5 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1033
• Residual factor for significantly intense reflections: 0.0631
• Weighted residual factors for significantly intense reflections: 0.1794
• Weighted residual factors for all reflections included in the refinement: 0.2035
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No