Information card for entry 7015591

Structure parameters

• Formula: B Bi Pb S4
• Calculated formula: B Bi Pb S4
• Title of publication: Syntheses, crystal structures and characterizations of two new quaternary thioborates: PbMBS4 (M = Sb, Bi).
• Authors of publication: Geng, Lei; Cheng, Wen-Dan; Zhang, Wei-Long; Li, Ye-Yu; Luo, Zhong-Zhen; Zhang, Hao; Lin, Chen-Sheng; He, Zhang-Zhen
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 17
• Pages of publication: 4474 - 4479
• a: 5.971 ± 0.01 Å
• b: 6.273 ± 0.009 Å
• c: 9.132 ± 0.015 Å
• α: 90°
• β: 107.75 ± 0.02°
• γ: 90°
• Cell volume: 325.8 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.043
• Residual factor for significantly intense reflections: 0.0355
• Weighted residual factors for significantly intense reflections: 0.0755
• Weighted residual factors for all reflections included in the refinement: 0.0791
• Goodness-of-fit parameter for all reflections included in the refinement: 1.141
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No