Synthesis, characterization, crystal structure and preliminary reactivity behaviour of new heteropolytopic ligands based on the 1,3,5-triazine spacer and pyrazolyl, tris-pyrazolylmethyl and tris-pyrazolylethoxy bonding fragments.
Authors of publication
Di Nicola, C.; Garau, F.; Marchetti, F.; Monari, M.; Pandolfo, L.; Pettinari, C.; Venzo, A.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2011
Journal volume
40
Journal issue
18
Pages of publication
4941 - 4953
a
19.6841 ± 0.0011 Å
b
11.6982 ± 0.0006 Å
c
12.5672 ± 0.0007 Å
α
90°
β
125.612 ± 0.001°
γ
90°
Cell volume
2352.6 ± 0.2 Å3
Cell temperature
298 ± 2 K
Ambient diffraction temperature
298 ± 2 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.048
Residual factor for significantly intense reflections
0.0441
Weighted residual factors for significantly intense reflections
0.1186
Weighted residual factors for all reflections included in the refinement
0.1229
Goodness-of-fit parameter for all reflections included in the refinement
