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Information card for entry 7015797
Preview
Coordinates | 7015797.cif |
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Original paper (by DOI) | HTML |
Formula | C42.25 H40.25 Cl11.75 P Pd |
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Calculated formula | C42.25 H40.25 Cl11.75 P Pd |
Title of publication | Cyclopropenylidene carbene ligands in palladium catalysed coupling reactions: carbene ligand rotation and application to the Stille reaction. |
Authors of publication | Chotima, Ratanon; Dale, Tim; Green, Michael; Hey, Thomas W.; McMullin, Claire L.; Nunns, Adam; Guy Orpen, A.; Shishkov, Igor V.; Wass, Duncan F.; Wingad, Richard L. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 19 |
Pages of publication | 5316 - 5323 |
a | 11.4288 ± 0.0006 Å |
b | 13.7141 ± 0.0008 Å |
c | 17.3825 ± 0.001 Å |
α | 94.734 ± 0.004° |
β | 106.928 ± 0.003° |
γ | 108.301 ± 0.003° |
Cell volume | 2428.8 ± 0.2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0832 |
Residual factor for significantly intense reflections | 0.0533 |
Weighted residual factors for significantly intense reflections | 0.1416 |
Weighted residual factors for all reflections included in the refinement | 0.1641 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71074 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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