Information card for entry 7015828

Structure parameters

• Formula: C40 H39 Br0.5 Cl1.5 N3 Ni P2
• Calculated formula: C40 H39 Br0.5 Cl1.5 N3 Ni P2
• Title of publication: Mononuclear and dinuclear palladium and nickel complexes of phosphinimine-based tridentate ligands.
• Authors of publication: Cariou, Renan; Dahcheh, Fatme; Graham, Todd W.; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 18
• Pages of publication: 4918 - 4925
• a: 12.0407 ± 0.0013 Å
• b: 22.977 ± 0.003 Å
• c: 13.459 ± 0.0014 Å
• α: 90°
• β: 97.437 ± 0.005°
• γ: 90°
• Cell volume: 3692.2 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0875
• Residual factor for significantly intense reflections: 0.0436
• Weighted residual factors for significantly intense reflections: 0.0878
• Weighted residual factors for all reflections included in the refinement: 0.1016
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No