Information card for entry 7015915

Structure parameters

• Formula: C36 H26 Cl2 N8 Rh2
• Calculated formula: C36 H26 Cl2 N8 Rh2
• SMILES: [Rh]1234([Rh]56(Cl)([c]72c(N=[N]1c1ccccc1)cccc7N=[N]5c1ccccc1)[c]14c(N=[N]3c2ccccc2)cccc1N=[N]6c1ccccc1)Cl
• Title of publication: Formation of organorhodium complexes via C-H bond activation of 1,3-di(phenylazo)benzene.
• Authors of publication: Majumder, Paramita; Baksi, Suparna; Halder, Sarmistha; Tadesse, Haregewine; Blake, Alexander J.; Drew, Michael G. B.; Bhattacharya, Samaresh
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 20
• Pages of publication: 5423 - 5425
• a: 15.3407 ± 0.0015 Å
• b: 13.3922 ± 0.0013 Å
• c: 19.085 ± 0.0019 Å
• α: 90°
• β: 103.245 ± 0.002°
• γ: 90°
• Cell volume: 3816.6 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0664
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0762
• Weighted residual factors for all reflections included in the refinement: 0.0819
• Goodness-of-fit parameter for all reflections included in the refinement: 0.84
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No