Information card for entry 7015954

Structure parameters

• Formula: C69 H43 B F20 Fe2 N2 Zn
• Calculated formula: C69 H38 B F20 Fe2 N2 Zn
• Title of publication: Reactions of Zn bis-ferrocenyl-β-diketiminates with [Ph(3)C][B(C(6)F(5))(4)].
• Authors of publication: Stanlake, Louisa J. E.; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 22
• Pages of publication: 5836 - 5840
• a: 12.8817 ± 0.0006 Å
• b: 15.2658 ± 0.0007 Å
• c: 17.4986 ± 0.0008 Å
• α: 75.639 ± 0.002°
• β: 68.973 ± 0.002°
• γ: 68.653 ± 0.002°
• Cell volume: 2964.2 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0585
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.1016
• Weighted residual factors for all reflections included in the refinement: 0.111
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No