Information card for entry 7016074

Structure parameters

• Formula: C37 H60 B Ca N3 O
• Calculated formula: C37 H60 B Ca N3 O
• Title of publication: Stoichiometric reactivity of dialkylamine boranes with alkaline earth silylamides.
• Authors of publication: Hill, Michael S.; Hodgson, Marina; Liptrot, David J.; Mahon, Mary F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 30
• Pages of publication: 7783 - 7790
• a: 16.784 ± 0.0003 Å
• b: 16.837 ± 0.0003 Å
• c: 26.359 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7448.8 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b n a
• Hall space group symbol: -P 2ac 2b
• Residual factor for all reflections: 0.1486
• Residual factor for significantly intense reflections: 0.0793
• Weighted residual factors for significantly intense reflections: 0.1921
• Weighted residual factors for all reflections included in the refinement: 0.2466
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No