Information card for entry 7016089

Structure parameters

• Formula: C34.86 H55.58 Cl0.14 N3 Ta
• Calculated formula: C34.86 H55.58 Cl0.14 N3 Ta
• Title of publication: Synthesis and reactivity of cationic niobium and tantalum methyl complexes supported by imido and β-diketiminato ligands.
• Authors of publication: Tomson, Neil C.; Arnold, John; Bergman, Robert G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 30
• Pages of publication: 7718 - 7729
• a: 10.4872 ± 0.0015 Å
• b: 13.1367 ± 0.0019 Å
• c: 24.997 ± 0.004 Å
• α: 90°
• β: 93.375 ± 0.002°
• γ: 90°
• Cell volume: 3437.8 ± 0.9 ų
• Cell temperature: 147 ± 2 K
• Ambient diffraction temperature: 147 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.054
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0739
• Weighted residual factors for all reflections included in the refinement: 0.0803
• Goodness-of-fit parameter for all reflections included in the refinement: 0.991
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No