Information card for entry 7016135

Structure parameters

• Formula: C20 H32 O6.84 P2
• Calculated formula: C20 H32 O6.836 P2
• Title of publication: Diphosphanes derived from phobane and phosphatrioxa-adamantane: similarities, differences and anomalies.
• Authors of publication: Dodds, Deborah L.; Floure, Joelle; Garland, Michael; Haddow, Mairi F.; Leonard, Thomas R.; McMullin, Claire L.; Orpen, A. Guy; Pringle, Paul G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 27
• Pages of publication: 7137 - 7146
• a: 13.019 ± 0.003 Å
• b: 8.4223 ± 0.0019 Å
• c: 20.509 ± 0.005 Å
• α: 90°
• β: 107.483 ± 0.012°
• γ: 90°
• Cell volume: 2144.9 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0621
• Residual factor for significantly intense reflections: 0.0396
• Weighted residual factors for significantly intense reflections: 0.0886
• Weighted residual factors for all reflections included in the refinement: 0.0968
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71074 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No