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Information card for entry 7016274
Preview
Coordinates | 7016274.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H34 F6 Fe N4 P2 |
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Calculated formula | C24 H34 F6 Fe N4 P2 |
SMILES | [Fe]12([N](=Cc3c(F)c(F)c(NC)c(F)c13)C)([N](=Cc1c(F)c(F)c(NC)c(F)c21)C)([P](C)(C)C)[P](C)(C)C |
Title of publication | Imine-assisted C-F bond activation by electron-rich iron complexes supported by trimethylphosphine. |
Authors of publication | Xu, Xiaofeng; Sun, Hongjian; Shi, Yujie; Jia, Jiong; Li, Xiaoyan |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 31 |
Pages of publication | 7866 - 7872 |
a | 10.4588 ± 0.001 Å |
b | 11.1141 ± 0.001 Å |
c | 14.4844 ± 0.0013 Å |
α | 96.805 ± 0.001° |
β | 93.337 ± 0.001° |
γ | 110.731 ± 0.001° |
Cell volume | 1554.4 ± 0.2 Å3 |
Cell temperature | 273 ± 2 K |
Ambient diffraction temperature | 273 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0369 |
Residual factor for significantly intense reflections | 0.0315 |
Weighted residual factors for significantly intense reflections | 0.0908 |
Weighted residual factors for all reflections included in the refinement | 0.0941 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.082 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7016274.html
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Users of the data should acknowledge the original authors of the
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