Information card for entry 7016305

Structure parameters

• Formula: C37 H40 Cl N Ni P2
• Calculated formula: C37 H40 Cl N Ni P2
• SMILES: c12c(cccc1)[P](c1ccccc1)(c1ccccc1)[Ni]1(Cl)N2c2c(cccc2)[P]1(C(C)C)C(C)C.Cc1ccccc1
• Title of publication: A terminal nickel(ii) anilide complex featuring an unsymmetrically substituted amido pincer ligand: synthesis and reactivity.
• Authors of publication: Liang, Lan-Chang; Li, Chun-Wei; Lee, Pei-Ying; Chang, Chih-Hsiang; Man Lee, Hon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 35
• Pages of publication: 9004 - 9011
• a: 12.365 ± 0.004 Å
• b: 15.097 ± 0.005 Å
• c: 18.987 ± 0.006 Å
• α: 110.914 ± 0.005°
• β: 92.567 ± 0.007°
• γ: 91.65 ± 0.006°
• Cell volume: 3303.7 ± 1.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1945
• Residual factor for significantly intense reflections: 0.0616
• Weighted residual factors for significantly intense reflections: 0.1268
• Weighted residual factors for all reflections included in the refinement: 0.1795
• Goodness-of-fit parameter for all reflections included in the refinement: 0.897
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No