Information card for entry 7016357

Structure parameters

• Formula: C30.5 H43 Cl O11 P2 Sn W
• Calculated formula: C30.5 H43 Cl O11 P2 Sn W
• Title of publication: Intramolecularly coordinated heteroleptic organostannylene tungsten pentacarbonyl complexes 4-tBu-2,6-[P(O)(OiPr)(2)](2)C(6)H(2)Sn(X)W(CO)(5) (X = Cl, F, PPh(2), PPh(2)[W(CO)(5)]). Syntheses and reactivity.
• Authors of publication: Wagner, Michael; Dorogov, Konstantin; Schürmann, Markus; Jurkschat, Klaus
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 35
• Pages of publication: 8839 - 8848
• a: 10.901 ± 0.002 Å
• b: 11.298 ± 0.002 Å
• c: 16.406 ± 0.003 Å
• α: 85.89 ± 0.03°
• β: 84.23 ± 0.03°
• γ: 78.72 ± 0.03°
• Cell volume: 1968.7 ± 0.7 ų
• Cell temperature: 173 ± 1 K
• Ambient diffraction temperature: 173 ± 1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0486
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for significantly intense reflections: 0.0456
• Weighted residual factors for all reflections included in the refinement: 0.0475
• Goodness-of-fit parameter for all reflections included in the refinement: 0.834
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No