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Information card for entry 7016403
Preview
Coordinates | 7016403.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C43 H64 Cl K2 O18 P Pd S2 |
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Calculated formula | C43 H64 Cl K2 O18 P Pd S2 |
Title of publication | Synthesis of non-symmetrically sulphonated phosphine sulphonate based Pd(ii) catalyst salts for olefin polymerisation reactions. |
Authors of publication | Anselment, Timo M. J.; Anderson, Carly E.; Rieger, Bernhard; Boeddinghaus, M. Bele; Fässler, Thomas F |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 33 |
Pages of publication | 8304 - 8313 |
a | 10.4999 ± 0.0009 Å |
b | 16.624 ± 0.001 Å |
c | 16.89 ± 0.001 Å |
α | 83.955 ± 0.004° |
β | 78.587 ± 0.004° |
γ | 79.133 ± 0.004° |
Cell volume | 2830.9 ± 0.3 Å3 |
Cell temperature | 110 ± 2 K |
Ambient diffraction temperature | 110 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1469 |
Residual factor for significantly intense reflections | 0.1088 |
Weighted residual factors for significantly intense reflections | 0.2304 |
Weighted residual factors for all reflections included in the refinement | 0.2383 |
Goodness-of-fit parameter for significantly intense reflections | 3.5 |
Goodness-of-fit parameter for all reflections included in the refinement | 2.84 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7016403.html
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