Information card for entry 7016407

Structure parameters

• Formula: C32 H26 Ni O4 P2
• Calculated formula: C32 H26 Ni O4 P2
• Title of publication: The impact of P-substituents on the structures, spectroscopic properties, and reactivities of POCOP-type pincer complexes of nickel(ii).
• Authors of publication: Salah, Abderrahmen B.; Zargarian, Davit
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 35
• Pages of publication: 8977 - 8985
• a: 8.7434 ± 0.0003 Å
• b: 9.9182 ± 0.0004 Å
• c: 16.1169 ± 0.0006 Å
• α: 92.699 ± 0.002°
• β: 97.355 ± 0.002°
• γ: 98.21 ± 0.002°
• Cell volume: 1368.89 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0738
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for significantly intense reflections: 0.1772
• Weighted residual factors for all reflections included in the refinement: 0.1866
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No