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Information card for entry 7016498
Preview
Coordinates | 7016498.cif |
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Original paper (by DOI) | HTML |
Formula | C38 H61 Fe5 N3 O14 |
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Calculated formula | C38.478 H61 Fe5 N3 O14 |
Title of publication | The chemistry of hydridocarbonylferrates revisited: syntheses and structures of the new [H(2)Fe(4)(CO)(12)](2-) and [HFe(5)(CO)(14)](3-) anions, and the [Fe(DMF)(4)][Fe(4)(CO)(12)(μ(5)-η(2)-CO)(μ-H)](2) adduct containing an unprecedented isocarbonyl. |
Authors of publication | Femoni, C.; Iapalucci, M. C.; Longoni, G.; Zacchini, S. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 34 |
Pages of publication | 8685 - 8694 |
a | 17.6836 ± 0.0014 Å |
b | 17.4956 ± 0.0014 Å |
c | 14.9768 ± 0.0012 Å |
α | 90° |
β | 91.788 ± 0.001° |
γ | 90° |
Cell volume | 4631.3 ± 0.6 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 5 |
Space group number | 12 |
Hermann-Mauguin space group symbol | C 1 2/m 1 |
Hall space group symbol | -C 2y |
Residual factor for all reflections | 0.0487 |
Residual factor for significantly intense reflections | 0.0373 |
Weighted residual factors for significantly intense reflections | 0.1015 |
Weighted residual factors for all reflections included in the refinement | 0.1131 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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