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Information card for entry 7016657
Preview
Coordinates | 7016657.cif |
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Original paper (by DOI) | HTML |
Formula | C41 H72 Mg2 N4 O2 Si4 |
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Calculated formula | C41 H64 Mg2 N4 O2 Si4 |
Title of publication | Crystalline metal (Li, Mg, Ca, Sr, Ba, Sn, Pb) complexes of the new chelating N,N'-dianionic [1,2-N(R)C(6)H(4)(CH(2)NR)](2-) ligand (R = SiMe(3), CH(2)Bu(t)). |
Authors of publication | Caro, Catherine F.; Coles, Martyn P.; Hitchcock, Peter B.; Lappert, Michael F.; Pierssens, Luc J.-M. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 38 |
Pages of publication | 9821 - 9830 |
a | 10.38 ± 0.005 Å |
b | 10.726 ± 0.003 Å |
c | 11.752 ± 0.004 Å |
α | 77.64 ± 0.02° |
β | 66.68 ± 0.03° |
γ | 82.2 ± 0.03° |
Cell volume | 1171.8 ± 0.8 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0586 |
Residual factor for significantly intense reflections | 0.047 |
Weighted residual factors for significantly intense reflections | 0.1229 |
Weighted residual factors for all reflections included in the refinement | 0.1305 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.058 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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