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Information card for entry 7016716
Preview
Coordinates | 7016716.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C55 H84 N6 Si4 Sm2 |
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Calculated formula | C54.5 H84 N6 Si4 Sm2 |
Title of publication | Synthesis, structure and catalytic activity of alkali metal-free bent-sandwiched lanthanide amido complexes with calix[4]-pyrrolyl ligands. |
Authors of publication | Zhou, Shuangliu; Wu, Shihong; Zhu, Hong; Wang, Shaowu; Zhu, Xiancui; Zhang, Lijun; Yang, Gaosheng; Cui, Daohui; Wang, Hengyu |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 37 |
Pages of publication | 9447 - 9453 |
a | 12.6353 ± 0.001 Å |
b | 29.185 ± 0.002 Å |
c | 19.4542 ± 0.0011 Å |
α | 90° |
β | 122.871 ± 0.004° |
γ | 90° |
Cell volume | 6025.4 ± 0.8 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1467 |
Residual factor for significantly intense reflections | 0.06 |
Weighted residual factors for significantly intense reflections | 0.0931 |
Weighted residual factors for all reflections included in the refinement | 0.1164 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.984 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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