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Information card for entry 7016725
Preview
Coordinates | 7016725.cif |
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Original paper (by DOI) | HTML |
Formula | C27 H41 Cl4 F3 N3 O3 P S |
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Calculated formula | C27 H41 Cl4 F3 N3 O3 P S |
Title of publication | Donor-stabilised cations, phosphinamide anions, and unusual oxidative cyclisation products from halogenated phosphoranimines and phosphinimines with a bulky 2,4,6-tri-tert-butylphenyl substituent at nitrogen. |
Authors of publication | Huynh, Keith; Chun, Cindy P.; Lough, Alan J.; Manners, Ian |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 40 |
Pages of publication | 10576 - 10584 |
a | 8.7008 ± 0.0002 Å |
b | 10.6081 ± 0.0003 Å |
c | 20.7723 ± 0.0006 Å |
α | 98.8 ± 0.0016° |
β | 90.99 ± 0.0018° |
γ | 112.465 ± 0.0015° |
Cell volume | 1744.88 ± 0.08 Å3 |
Cell temperature | 150 ± 1 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0808 |
Residual factor for significantly intense reflections | 0.0492 |
Weighted residual factors for significantly intense reflections | 0.1194 |
Weighted residual factors for all reflections included in the refinement | 0.1391 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.031 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7016725.html
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Users of the data should acknowledge the original authors of the
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