Crystallography Open Database

Information card for entry 7016760

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Coordinates	7016760.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H37 N Si
Calculated formula	C36 H37 N Si
Title of publication	Extremely bulky amido-group 14 element chloride complexes: Potential synthons for low oxidation state main group chemistry.
Authors of publication	Li, Jiaye; Stasch, Andreas; Schenk, Christian; Jones, Cameron
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2011
Journal volume	40
Journal issue	40
Pages of publication	10448 - 10456
a	16.6936 ± 0.0008 Å
b	22.4261 ± 0.0009 Å
c	7.639 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	2859.8 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0797
Residual factor for significantly intense reflections	0.0491
Weighted residual factors for significantly intense reflections	0.1049
Weighted residual factors for all reflections included in the refinement	0.1185
Goodness-of-fit parameter for all reflections included in the refinement	1.064
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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