Information card for entry 7016762

Structure parameters

• Formula: C36 H36 Cl3 N Si2
• Calculated formula: C36 H36 Cl3 N Si2
• Title of publication: Extremely bulky amido-group 14 element chloride complexes: Potential synthons for low oxidation state main group chemistry.
• Authors of publication: Li, Jiaye; Stasch, Andreas; Schenk, Christian; Jones, Cameron
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 40
• Pages of publication: 10448 - 10456
• a: 10.0788 ± 0.0007 Å
• b: 13.1075 ± 0.0009 Å
• c: 13.1687 ± 0.0009 Å
• α: 90.754 ± 0.003°
• β: 108.006 ± 0.004°
• γ: 96.141 ± 0.004°
• Cell volume: 1643 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0533
• Residual factor for significantly intense reflections: 0.0476
• Weighted residual factors for significantly intense reflections: 0.0997
• Weighted residual factors for all reflections included in the refinement: 0.1021
• Goodness-of-fit parameter for all reflections included in the refinement: 1.197
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No