Crystallography Open Database

Information card for entry 7016764

Preview

Coordinates	7016764.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H37 Cl2 N Si2
Calculated formula	C36 H37 Cl2 N Si2
Title of publication	Extremely bulky amido-group 14 element chloride complexes: Potential synthons for low oxidation state main group chemistry.
Authors of publication	Li, Jiaye; Stasch, Andreas; Schenk, Christian; Jones, Cameron
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2011
Journal volume	40
Journal issue	40
Pages of publication	10448 - 10456
a	12.508 ± 0.0007 Å
b	17.046 ± 0.001 Å
c	15.5962 ± 0.0009 Å
α	90°
β	97.4 ± 0.002°
γ	90°
Cell volume	3297.6 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1175
Residual factor for significantly intense reflections	0.081
Weighted residual factors for significantly intense reflections	0.1998
Weighted residual factors for all reflections included in the refinement	0.2215
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7016764.html