Information card for entry 7016859

Structure parameters

• Formula: C24 H25 F6 N3 O7 S2 Si
• Calculated formula: C24 H25 F6 N3 O7 S2 Si
• Title of publication: Novel neutral hexacoordinate benzamidinatosilicon(iv) complexes with SiN(3)OF(2), SiN(3)OCl(2), SiN(3)OBr(2), SiN(5)O and SiN(3)O(3) skeletons.
• Authors of publication: Junold, Konstantin; Burschka, Christian; Bertermann, Rüdiger; Tacke, Reinhold
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 38
• Pages of publication: 9844 - 9857
• a: 23.2733 ± 0.0016 Å
• b: 16.3163 ± 0.001 Å
• c: 30.8 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11695.8 ± 1.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0596
• Residual factor for significantly intense reflections: 0.0439
• Weighted residual factors for significantly intense reflections: 0.1138
• Weighted residual factors for all reflections included in the refinement: 0.1211
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No