Information card for entry 7016873

Structure parameters

• Formula: C71 H62 Cl12 Fe4 O4 P4
• Calculated formula: C71 H62 Cl12 Fe4 O4 P4
• Title of publication: Complexation of 1,1'-bis(diphenylphosphino)ferrocene dioxide (dppfO(2)) with 3d metals and revisit of its coordination to Pd(ii).
• Authors of publication: Zhang, Wenhua; Hor, T. S. Andy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 40
• Pages of publication: 10725 - 10730
• a: 13.3325 ± 0.0007 Å
• b: 18.2129 ± 0.001 Å
• c: 32.9846 ± 0.0018 Å
• α: 74.715 ± 0.001°
• β: 84.37 ± 0.001°
• γ: 78.428 ± 0.001°
• Cell volume: 7560.4 ± 0.7 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1126
• Residual factor for significantly intense reflections: 0.0824
• Weighted residual factors for significantly intense reflections: 0.1997
• Weighted residual factors for all reflections included in the refinement: 0.2151
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No