Information card for entry 7016879

Structure parameters

• Formula: C34 H28 Br2 Co Fe O2 P2
• Calculated formula: C34 H28 Br2 Co Fe O2 P2
• Title of publication: Complexation of 1,1'-bis(diphenylphosphino)ferrocene dioxide (dppfO(2)) with 3d metals and revisit of its coordination to Pd(ii).
• Authors of publication: Zhang, Wenhua; Hor, T. S. Andy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 40
• Pages of publication: 10725 - 10730
• a: 10.1369 ± 0.0006 Å
• b: 19.6944 ± 0.0012 Å
• c: 16.1275 ± 0.001 Å
• α: 90°
• β: 91.483 ± 0.001°
• γ: 90°
• Cell volume: 3218.6 ± 0.3 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0511
• Residual factor for significantly intense reflections: 0.0442
• Weighted residual factors for significantly intense reflections: 0.1031
• Weighted residual factors for all reflections included in the refinement: 0.1072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No