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Information card for entry 7017035
Preview
Coordinates | 7017035.cif |
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Original paper (by DOI) | HTML |
Formula | C22 H26 B Cl4 F4 N4 O4 Rh3 S2 |
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Calculated formula | C22 H26 B Cl4 F4 N4 O4 Rh3 S2 |
Title of publication | The oxidative conversion of the N,S-bridged complexes [{RhLL'(μ-X)}(2)] to [(RhLL')(3)(μ-X)(2)](+) (X = mt or taz): a comparison with the oxidation of N,N-bridged analogues. |
Authors of publication | Blagg, Robin J.; López-Gómez, María J; Charmant, Jonathan P. H.; Connelly, Neil G.; Cowell, John J.; Haddow, Mairi F.; Hamilton, Alex; Orpen, A. Guy; Riis-Johannessen, Thomas; Saithong, Saowanit |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 43 |
Pages of publication | 11497 - 11510 |
a | 10.979 ± 0.002 Å |
b | 13.334 ± 0.003 Å |
c | 13.909 ± 0.003 Å |
α | 99.01 ± 0.03° |
β | 109 ± 0.03° |
γ | 114.02 ± 0.03° |
Cell volume | 1657.1 ± 1 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 9 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0876 |
Residual factor for significantly intense reflections | 0.081 |
Weighted residual factors for significantly intense reflections | 0.2144 |
Weighted residual factors for all reflections included in the refinement | 0.2188 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.168 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7017035.html
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