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Information card for entry 7017332
Preview
Coordinates | 7017332.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H33 Cl2 N3 Ni O |
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Calculated formula | C24 H33 Cl2 N3 Ni O |
SMILES | [Ni]12(Cl)(Cl)[n]3c(cccc3C(=[N]2c2c(C(C)C)cccc2C(C)C)C)C(=[O]1)NCCCC |
Title of publication | 2-(N-Alkylcarboxamide)-6-iminopyridyl palladium and nickel complexes: coordination chemistry and catalysis. |
Authors of publication | Zhang, Wenjuan; Wang, Youhong; Yu, Jiangang; Redshaw, Carl; Hao, Xiang; Sun, Wen-Hua |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2011 |
Journal volume | 40 |
Journal issue | 48 |
Pages of publication | 12856 - 12865 |
a | 10.797 ± 0.002 Å |
b | 16.923 ± 0.003 Å |
c | 13.86 ± 0.003 Å |
α | 90° |
β | 92.19 ± 0.03° |
γ | 90° |
Cell volume | 2530.6 ± 0.9 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1328 |
Residual factor for significantly intense reflections | 0.0679 |
Weighted residual factors for significantly intense reflections | 0.1514 |
Weighted residual factors for all reflections included in the refinement | 0.1743 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.913 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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