Information card for entry 7017343

Structure parameters

• Formula: C32 H39 Br Cl2 N3 P
• Calculated formula: C32 H39 Br Cl2 N3 P
• Title of publication: Substitution matters: isolating phosphorus diiminopyridine complexes.
• Authors of publication: Martin, Caleb D.; Ragogna, Paul J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 44
• Pages of publication: 11976 - 11980
• a: 17.049 ± 0.003 Å
• b: 13.12 ± 0.003 Å
• c: 17.259 ± 0.004 Å
• α: 90°
• β: 119.39 ± 0.03°
• γ: 90°
• Cell volume: 3363.7 ± 1.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0944
• Residual factor for significantly intense reflections: 0.0606
• Weighted residual factors for significantly intense reflections: 0.1691
• Weighted residual factors for all reflections included in the refinement: 0.2018
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No