Crystallography Open Database

Information card for entry 7017356

Preview

Coordinates	7017356.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25.5 H30 Cl2 N3 O Re
Calculated formula	C25.5 H30 Cl2 N3 O Re
Title of publication	Synthesis and characterization of oxorhenium(v) diamido pyridine complexes that catalyze oxygen atom transfer reactions.
Authors of publication	Lilly, Cassandra P.; Boyle, Paul D.; Ison, Elon A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2011
Journal volume	40
Journal issue	44
Pages of publication	11815 - 11821
a	9.6153 ± 0.0005 Å
b	11.9246 ± 0.0006 Å
c	12.6634 ± 0.0006 Å
α	63.761 ± 0.002°
β	73.053 ± 0.002°
γ	81.327 ± 0.002°
Cell volume	1245.39 ± 0.11 Å³
Cell temperature	110 K
Ambient diffraction temperature	110 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0311
Residual factor for significantly intense reflections	0.0255
Weighted residual factors for significantly intense reflections	0.0555
Weighted residual factors for all reflections included in the refinement	0.0569
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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