Information card for entry 7017369

Structure parameters

• Formula: C62.25 H54.5 Cl6.5 N2 P4 S2 W
• Calculated formula: C62.25 H49.3333 Cl6.5 N2 P4 S2 W
• Title of publication: Transformations of aryl isothiocyanates on tetraphosphine tungsten complexes and reactivity of the resulting dithiocarbonimidate ligand.
• Authors of publication: Dai, Qi Xiu; Seino, Hidetake; Mizobe, Yasushi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 44
• Pages of publication: 11822 - 11830
• a: 19.16 ± 0.002 Å
• b: 21.884 ± 0.002 Å
• c: 24.197 ± 0.003 Å
• α: 81.904 ± 0.004°
• β: 88.235 ± 0.004°
• γ: 69.704 ± 0.003°
• Cell volume: 9419.2 ± 1.8 ų
• Cell temperature: 113.1 K
• Ambient diffraction temperature: 113.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0657
• Weighted residual factors for all reflections included in the refinement: 0.1927
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No