Information card for entry 7017371

Structure parameters

• Formula: C65 H63 Cl4 I N2 P4 S2 W
• Calculated formula: C65 H59 Cl4 I N2 P4 S2 W
• Title of publication: Transformations of aryl isothiocyanates on tetraphosphine tungsten complexes and reactivity of the resulting dithiocarbonimidate ligand.
• Authors of publication: Dai, Qi Xiu; Seino, Hidetake; Mizobe, Yasushi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 44
• Pages of publication: 11822 - 11830
• a: 17.357 ± 0.003 Å
• b: 11.468 ± 0.002 Å
• c: 32.634 ± 0.006 Å
• α: 90°
• β: 104.098 ± 0.0007°
• γ: 90°
• Cell volume: 6300.2 ± 1.9 ų
• Cell temperature: 113.1 K
• Ambient diffraction temperature: 113.1 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0556
• Weighted residual factors for all reflections included in the refinement: 0.1541
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No