Information card for entry 7017594

Structure parameters

• Formula: C22 H24 N2 O15 Pb S4
• Calculated formula: C22 H20 N2 O13 Pb S4
• Title of publication: 2D sheet-like architectures constructed from main-group metal ions, 4,4'-bpno and 1,2-alternate p-sulfonatothiacalix[4]arene.
• Authors of publication: Xiong, Kecai; Jiang, Feilong; Yang, Ming; Wu, Mingyan; Feng, Rui; Xu, Wentao; Hong, Maochun
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 2
• Pages of publication: 540 - 545
• a: 8.729 ± 0.003 Å
• b: 11.682 ± 0.004 Å
• c: 15.591 ± 0.005 Å
• α: 98.598 ± 0.004°
• β: 90.922 ± 0.002°
• γ: 110.883 ± 0.004°
• Cell volume: 1464.6 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0603
• Residual factor for significantly intense reflections: 0.0495
• Weighted residual factors for significantly intense reflections: 0.1066
• Weighted residual factors for all reflections included in the refinement: 0.1146
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No