Information card for entry 7017598

Structure parameters

• Formula: C52 H144 B30 Mo2 N8 O6 Sn6
• Calculated formula: C52 H144 B30 Mo2 N8 O6 Sn6
• Title of publication: 1,2-Distanna-closo-dodecaborate‒a rare example of a 1,2-distannylene ligand in transition metal chemistry.
• Authors of publication: Nickl, Claudia; Eichele, Klaus; Wesemann, Lars
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 1
• Pages of publication: 243 - 250
• a: 15.5311 ± 0.0012 Å
• b: 20.8394 ± 0.0015 Å
• c: 15.9241 ± 0.0013 Å
• α: 90°
• β: 117.951 ± 0.005°
• γ: 90°
• Cell volume: 4552.8 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.139
• Residual factor for significantly intense reflections: 0.0813
• Weighted residual factors for significantly intense reflections: 0.1457
• Weighted residual factors for all reflections included in the refinement: 0.1711
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No