Crystallography Open Database

Information card for entry 7017601

Preview

Coordinates	7017601.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C90 H85 Au2 B10 N3 P6 Sn2
Calculated formula	C90 H85 Au2 B10 N3 P6 Sn2
Title of publication	1,2-Distanna-closo-dodecaborate‒a rare example of a 1,2-distannylene ligand in transition metal chemistry.
Authors of publication	Nickl, Claudia; Eichele, Klaus; Wesemann, Lars
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	1
Pages of publication	243 - 250
a	12.8328 ± 0.001 Å
b	17.404 ± 0.0012 Å
c	21.9546 ± 0.0017 Å
α	70.017 ± 0.006°
β	75.399 ± 0.006°
γ	75.306 ± 0.006°
Cell volume	4383.1 ± 0.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0993
Residual factor for significantly intense reflections	0.0629
Weighted residual factors for significantly intense reflections	0.0856
Weighted residual factors for all reflections included in the refinement	0.0939
Goodness-of-fit parameter for all reflections included in the refinement	1.109
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7017601.html