Information card for entry 7017645

Structure parameters

• Formula: C26 H16 F24 N2
• Calculated formula: C26 H16 F24 N2
• Title of publication: Electrochemical nickel-induced fluoroalkylation: synthetic, structural and mechanistic study.
• Authors of publication: Mikhaylov, Dmitry; Gryaznova, Tatyana; Dudkina, Yulia; Khrizanphorov, Mikhail; Latypov, Shamil; Kataeva, Olga; Vicic, David A.; Sinyashin, Oleg G.; Budnikova, Yulia
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 1
• Pages of publication: 165 - 172
• a: 16.091 ± 0.001 Å
• b: 5.905 ± 0.001 Å
• c: 16.645 ± 0.001 Å
• α: 90°
• β: 110.047 ± 0.005°
• γ: 90°
• Cell volume: 1485.7 ± 0.3 ų
• Cell temperature: 198 ± 2 K
• Ambient diffraction temperature: 198 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0571
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.0966
• Weighted residual factors for all reflections included in the refinement: 0.1058
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No